Molecular structure studies of (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol

Tao Zhang; Krzysztof Paluch; Gaia Scalabrino; Neil Frankish; Anne Marie Healy; Helen Sheridan

doi:10.1016/j.molstruc.2014.12.018

Molecular structure studies of (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol

Tao Zhang, Krzysztof Paluch, Gaia Scalabrino, Neil Frankish, Anne Marie Healy, Helen Sheridan

Research output: Contribution to journal › Article › peer-review

Abstract

The single enantiomer (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol (2), has recently been synthesized and isolated from its corresponding diastereoisomer (1). The molecular and crystal structures of this novel compound have been fully analyzed. The relative and absolute configurations have been determined by using a combination of analytical tools including X-ray crystallography, X-ray Powder Diffraction (XRPD) analysis and Nuclear Magnetic Resonance (NMR) spectroscopy.

Original language	English
Pages (from-to)	286-299
Number of pages	14
Journal	Journal of Molecular Structure
Volume	1083
DOIs	https://doi.org/10.1016/j.molstruc.2014.12.018
Publication status	Published - 5 Mar 2015
Externally published	Yes

Keywords

(1S 2S)-2-Benzyl-2 3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol
Chemical separation
NMR X-ray
Single enantiomer
XRPD

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10.1016/j.molstruc.2014.12.018

https://arrow.tudublin.ie/schfsehart/356Licence: CC BY-NC-SA

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title = "Molecular structure studies of (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol",

abstract = "The single enantiomer (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol (2), has recently been synthesized and isolated from its corresponding diastereoisomer (1). The molecular and crystal structures of this novel compound have been fully analyzed. The relative and absolute configurations have been determined by using a combination of analytical tools including X-ray crystallography, X-ray Powder Diffraction (XRPD) analysis and Nuclear Magnetic Resonance (NMR) spectroscopy.",

keywords = "(1S 2S)-2-Benzyl-2 3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol, Chemical separation, NMR X-ray, Single enantiomer, XRPD",

author = "Tao Zhang and Krzysztof Paluch and Gaia Scalabrino and Neil Frankish and Healy, {Anne Marie} and Helen Sheridan",

note = "Publisher Copyright: {\textcopyright} 2014 The Authors. Published by Elsevier B.V.",

year = "2015",

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doi = "10.1016/j.molstruc.2014.12.018",

language = "English",

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AU - Zhang, Tao

AU - Paluch, Krzysztof

AU - Scalabrino, Gaia

AU - Frankish, Neil

AU - Healy, Anne Marie

AU - Sheridan, Helen

PY - 2015/3/5

Y1 - 2015/3/5

N2 - The single enantiomer (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol (2), has recently been synthesized and isolated from its corresponding diastereoisomer (1). The molecular and crystal structures of this novel compound have been fully analyzed. The relative and absolute configurations have been determined by using a combination of analytical tools including X-ray crystallography, X-ray Powder Diffraction (XRPD) analysis and Nuclear Magnetic Resonance (NMR) spectroscopy.

AB - The single enantiomer (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol (2), has recently been synthesized and isolated from its corresponding diastereoisomer (1). The molecular and crystal structures of this novel compound have been fully analyzed. The relative and absolute configurations have been determined by using a combination of analytical tools including X-ray crystallography, X-ray Powder Diffraction (XRPD) analysis and Nuclear Magnetic Resonance (NMR) spectroscopy.

KW - (1S 2S)-2-Benzyl-2 3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol

KW - Chemical separation

KW - NMR X-ray

KW - Single enantiomer

KW - XRPD

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ER -

Molecular structure studies of (1S,2S)-2-benzyl-2,3-dihydro-2-(1H-inden-2-yl)-1H-inden-1-ol

Abstract

Keywords

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